Mahmood F. Chawshli; Shakhawan K.  Hamad

doi:10.14715/cmb/2023.69.10.39

Issue

Vol. 69 No. 10: Issue 10

Issue Published : October 31, 2023

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Novel Core-shell Bioceramic Silica-Berberis vulgaris: Synthesis and Characterization

synthesis of Bioceramic Silica-Berberis core-shell

https://doi.org/10.14715/cmb/2023.69.10.39

Mahmood F. Chawshli

Conservative Department, Hawler Medical University, Erbil 44000, Iraq

Shakhawan K. Hamad

Conservative Department, Hawler Medical University, Erbil 44000, Iraq

Corresponding Author(s) : Mahmood F. Chawshli

dentist.mahmood@gmail.com

Cellular and Molecular Biology, Vol. 69 No. 10: Issue 10
Article Published : October 31, 2023

Abstract

Enhancements in bioceramic mixtures represent a significant avenue for achieving superior mechanical and biological properties. Therefore, the present study aimed to extract active compounds from Berberis vulgaris stems and fruits collected from the Khorasan province, employing advanced analytical techniques such as GC-MS and FTIR to elucidate the composition of these extracts. The derived extracts were utilized to synthesize novel nanocomposites, denoted as SiO₂-MPS-stem extract and SiO₂-MPS-fruit extract. Comprehensive Characterization of these composites was conducted through SEM, EDX mapping, FTIR, and XRD analyses. The characterization measurements validated the successful coating of silica with the extracts, resulting in a core-shell nanostructure with particle sizes below 60 nm. These composites were incorporated into bioceramics for dental root fillings with an equal weight ratio. The bioceramic material was subjected to the same aforementioned characterization techniques, revealing that their sizes fell within the nanoscale range, not exceeding 70 nanometers. The results indicated a core-shell configuration for the nanomaterials, with the shell comprising the bioceramic component of bioceramic-SiO₂-MPS-fruit extract and bioceramic-SiO₂-MPS-stem extract.

Keywords

Keywords: Bioceramic mixtures; stem extract; fruit extract; core-shell nanostructure; dental root fillings.

Chawshli, M. F., & Hamad, S. K. . (2023). Novel Core-shell Bioceramic Silica-Berberis vulgaris: Synthesis and Characterization : synthesis of Bioceramic Silica-Berberis core-shell. Cellular and Molecular Biology, 69(10), 264–275. https://doi.org/10.14715/cmb/2023.69.10.39